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Towards new binary compounds: Synthesis of amorphous phosphorus carbide by pulsed laser deposition

Identifieur interne : 000301 ( Main/Repository ); précédent : 000300; suivant : 000302

Towards new binary compounds: Synthesis of amorphous phosphorus carbide by pulsed laser deposition

Auteurs : RBID : Pascal:13-0133860

Descripteurs français

Pascal (Inist)
- Composé binaire, Phosphore, Dépôt laser pulsé, Méthode ablation laser, Structure cristalline, Couche mince amorphe, Structure locale, Carbone, Spectre photoélectron RX, Sulfure d'indium, 8115F, 6166.
Wicri :
- concept : Phosphore, Carbone.

English descriptors

KwdEn :
- Amorphous thin film, Binary compounds, Carbon, Crystal structure, Indium sulfide, Laser ablation technique, Local structure, Phosphorus, Pulsed laser deposition, X-ray photoelectron spectra.

Abstract

We have recently undertaken comprehensive computational studies predicting possible crystal structures of the as yet unknown phosphorus carbide as a function of composition. In this work, we report the synthesis of amorphous phosphorus-carbon films by pulsed laser deposition. The local bonding environments of carbon and phosphorus in the synthesised materials have been analysed by x-ray photoelectron spectroscopy; we have found strong evidence for the formation of direct P-C bonding and hence phosphorus carbide. There is a good agreement between the bonding environments found in this phosphorus carbide material and those predicted in the computational work. In particular, the local bonding environments are consistent with those found in the β-InS-like structures that we predict to be low in energy for phosphorus:carbon ratios between 0.25 and 1.

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Pascal:13-0133860

Le document en format XML

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<author><name sortKey="Hart, Judy N" uniqKey="Hart J">Judy N. Hart</name>
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<country>Royaume-Uni</country>
<wicri:noRegion>Bristol BS8 ITS</wicri:noRegion>
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<author><name sortKey="May, Paul W" uniqKey="May P">Paul W. May</name>
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<author><name sortKey="Allan, Neil L" uniqKey="Allan N">Neil L. Allan</name>
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<country>Royaume-Uni</country>
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<author><name sortKey="Hallam, Keith R" uniqKey="Hallam K">Keith R. Hallam</name>
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<author><name sortKey="Claeyssens, Frederik" uniqKey="Claeyssens F">Frederik Claeyssens</name>
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<author><name sortKey="Fuge, Gareth M" uniqKey="Fuge G">Gareth M. Fuge</name>
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<author><name sortKey="Ruda, Michelle" uniqKey="Ruda M">Michelle Ruda</name>
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<author><name sortKey="Heard, Peter J" uniqKey="Heard P">Peter J. Heard</name>
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<publicationStmt><idno type="inist">13-0133860</idno>
<date when="2013">2013</date>
<idno type="stanalyst">PASCAL 13-0133860 INIST</idno>
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<term>Crystal structure</term>
<term>Indium sulfide</term>
<term>Laser ablation technique</term>
<term>Local structure</term>
<term>Phosphorus</term>
<term>Pulsed laser deposition</term>
<term>X-ray photoelectron spectra</term>
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<keywords scheme="Pascal" xml:lang="fr"><term>Composé binaire</term>
<term>Phosphore</term>
<term>Dépôt laser pulsé</term>
<term>Méthode ablation laser</term>
<term>Structure cristalline</term>
<term>Couche mince amorphe</term>
<term>Structure locale</term>
<term>Carbone</term>
<term>Spectre photoélectron RX</term>
<term>Sulfure d'indium</term>
<term>8115F</term>
<term>6166</term>
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<keywords scheme="Wicri" type="concept" xml:lang="fr"><term>Phosphore</term>
<term>Carbone</term>
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<front><div type="abstract" xml:lang="en">We have recently undertaken comprehensive computational studies predicting possible crystal structures of the as yet unknown phosphorus carbide as a function of composition. In this work, we report the synthesis of amorphous phosphorus-carbon films by pulsed laser deposition. The local bonding environments of carbon and phosphorus in the synthesised materials have been analysed by x-ray photoelectron spectroscopy; we have found strong evidence for the formation of direct P-C bonding and hence phosphorus carbide. There is a good agreement between the bonding environments found in this phosphorus carbide material and those predicted in the computational work. In particular, the local bonding environments are consistent with those found in the β-InS-like structures that we predict to be low in energy for phosphorus:carbon ratios between 0.25 and 1.</div>
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<fA08 i1="01" i2="1" l="ENG"><s1>Towards new binary compounds: Synthesis of amorphous phosphorus carbide by pulsed laser deposition</s1>
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<fA11 i1="01" i2="1"><s1>HART (Judy N.)</s1>
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<fA11 i1="02" i2="1"><s1>MAY (Paul W.)</s1>
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<fA11 i1="03" i2="1"><s1>ALLAN (Neil L.)</s1>
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<fA11 i1="04" i2="1"><s1>HALLAM (Keith R.)</s1>
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<fA11 i1="08" i2="1"><s1>HEARD (Peter J.)</s1>
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<sZ>3 aut.</sZ>
<sZ>6 aut.</sZ>
<sZ>7 aut.</sZ>
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<sZ>8 aut.</sZ>
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<fC01 i1="01" l="ENG"><s0>We have recently undertaken comprehensive computational studies predicting possible crystal structures of the as yet unknown phosphorus carbide as a function of composition. In this work, we report the synthesis of amorphous phosphorus-carbon films by pulsed laser deposition. The local bonding environments of carbon and phosphorus in the synthesised materials have been analysed by x-ray photoelectron spectroscopy; we have found strong evidence for the formation of direct P-C bonding and hence phosphorus carbide. There is a good agreement between the bonding environments found in this phosphorus carbide material and those predicted in the computational work. In particular, the local bonding environments are consistent with those found in the β-InS-like structures that we predict to be low in energy for phosphorus:carbon ratios between 0.25 and 1.</s0>
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<fC03 i1="02" i2="3" l="FRE"><s0>Phosphore</s0>
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<s5>02</s5>
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<s5>02</s5>
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<s5>03</s5>
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<s5>04</s5>
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<s5>04</s5>
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<s5>05</s5>
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<s5>05</s5>
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<s5>06</s5>
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<s5>06</s5>
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<s5>15</s5>
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<fC03 i1="11" i2="3" l="FRE"><s0>8115F</s0>
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Towards new binary compounds: Synthesis of amorphous phosphorus carbide by pulsed laser deposition

Towards new binary compounds: Synthesis of amorphous phosphorus carbide by pulsed laser deposition

Descripteurs français

English descriptors

Abstract

Links toward previous steps (curation, corpus...)

Links to Exploration step

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

Pour mettre un lien sur cette page dans le réseau Wicri